Determination of inorganic arsenic in feed and food by HPLC-ICPMS
14-16 May 2024
The training focused on the two CEN methods EN 16802:2016 (Determination of inorganic arsenic in foodstuffs of marine and plant origin by anion-exchange HPLC-ICP-MS) and EN 17374:2020 (Determination of inorganic arsenic in animal feed by anion-exchange HPLC-ICPMS). The training included both theoretical and practical sessions.
Learning objectives
Introduction to the determination of inorganic arsenic in feed and food by HPLC-ICP-MS. The participants were expected to gain enough knowledge to be able to set up the methodology in their own laboratory following the training. The training consisted of both theoretical and practical sessions focused on the two CEN methods EN 16802:2016 (Determination of inorganic arsenic in foodstuffs of marine and plant origin by anion-exchange HPLC-ICP-MS) and EN 17374:2020 (Determination of inorganic arsenic in animal feed by anion-exchange HPLC-ICP-MS).
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Tuesday
14 May 2024
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Wednesday
15 May 2024
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Thursday
16 May 2023
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9:00
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Welcome
Introduction of participants
Introduction of the training
NRLs; experience and plans
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Lab work – Analysis
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Data analysis
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Lectures
- Introduction – Arsenic in feed and food, legislation, speciation analysis
- CEN methods - Background, sample preparation
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10:30
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Coffee break
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Coffee break
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Coffee break
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11:00
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Lectures
- CEN method, Separation, Detection
- Introduction lab work, including safety
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Lab work – Analysis
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Q&A
PTs – results and challenges
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12:00
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Lunch
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Lunch
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Lunch
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13:00
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Lab work
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Lab work; Analysis
- Prepare sequence
- Analyse samples
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Goodbyes
End of day 3
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15:00
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Coffee break
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Coffee break
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15:15
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Lab work
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Lab work; Analysis
Lectures:
- HPLC requirements
- Quality assurance
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17:00
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End of day 1
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End of day 2
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19:00
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Dinner
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